Scanning Electron Microscopy

The scanning electron microscope (SEM) is one of the most versatile pieces of equipment currently available for geological analysis and offers a wide range of imaging and analytical modes, several of which are illustrated here. More recently the SEM has become synonymous with petrofabric analysis via the technique of electron backscattered diffraction (EBSD), which has largely superceded the earlier SEM-based approach using the electron channelling (EC) effect. Click on the appropriate thumb-nail sketch for the complete image and further details on that particular SEM technique.
 
semconfig.jpg (52768 bytes) Schematic SEM set up. Secondary electron imageSecondary electron image
Atomic number (Z) contrastAtomic number (Z) contrast ecoc1.jpg (73777 bytes)Electron channelling (EC) orientation contrast (OC).
eg_ecp.jpg (17969 bytes)Electron channelling pattern (ECP). globe.jpg (81862 bytes)Original ECP indexing. 
eg_ebsp.jpg (20513 bytes)Electron Backscattered Diffraction Pattern (EBSP). uncoated.jpg (92697 bytes)Examples of EBSD OC (FSE) images.
qtzebsd.jpg (45800 bytes)EBSP indexing.  automated EBSD analysisg110800.jpg (164179 bytes)Example of automated EBSD analysis.
combebsp.jpg (78262 bytes)EBSP indexing problems I: pattern superposition.  qtzpseudsymm.jpg (102595 bytes)EBSP indexing problems II: pseudosymmetry. 
aug_pigEBSP indexing problems III: similarities in crystal structures and/or mineral composition. CathodoluminescenceCathodoluminescence